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·인용수 1
·2024
Glycoside-metabolizing oxidoreductase D3dgpA from human gut bacterium
Heji Kim, Huỳnh Thị Ngọc Mi, Joong‐Hoon Ahn, Jong Suk Lee, Bekir Engin Eser, Jongkeun Choi, Jaehong Han
IF 4.8Frontiers in Bioengineering and Biotechnology
초록

The Gfo/Idh/MocA family enzyme DgpA was known to catalyze the regiospecific oxidation of puerarin to 3"-oxo-puerarin in the presence of 3-oxo-glucose. Here, we discovered that D3dgpA, <i>dgpA</i> cloned from the human gut bacterium <i>Dorea</i> sp. MRG-IFC3, catalyzed the regiospecific oxidation of various <i>C</i>-/<i>O</i>-glycosides, including puerarin, in the presence of methyl β-D-3-oxo-glucopyranoside. While <i>C</i>-glycosides were converted to 3"- and 2"-oxo-products by D3dgpA, <i>O</i>-glycosides resulted in the formation of aglycones and hexose enediolone from the 3"-oxo-products. From DFT calculations, it was found that isomerization of 3"-oxo-puerarin to 2"-oxo-puerarin required a small activation energy of 9.86 kcal/mol, and the <i>O</i>-glycosidic bond cleavage of 3"-oxo-products was also thermodynamically favored with a small activation energy of 3.49 kcal/mol. In addition, the reaction mechanism of D3dgpA was discussed in comparison to those of Gfo/Idh/MocA and GMC family enzymes. The robust reactivity of D3dgpA was proposed as a new general route for derivatization of glycosides.

키워드
OxidoreductaseGlycosideBacteriaMicrobiologyBiologyChemistryBiochemistryStereochemistryEnzymeGenetics
타입
article
IF / 인용수
4.8 / 1
게재 연도
2024